Spray Pyrolysis Technique for the Deposition of Lead Oxide (PbO) Thin Films; its Electrochemical Behaviour and Structural and Optical Properties

eng Oriental Scientific Publishing Company Material Science Research India 0973-3469 2018-08-25 15 2 134 140 8060 article Spray Pyrolysis Technique for the Deposition of Lead Oxide (PbO) Thin Films; its Electrochemical Behaviour and Structural and Optical Properties Anil B Gite 1 G. E. Patil 1 G. H. Jain 1 SNJB’s Department of Physics, Arts Commerce and Science College Chandwad Nashik, Maharashtra, India

Thin film of Lead oxide (PbO) was prepared by spray pyrolysis technique on glass substrate at 250^°C. The cyclic voltammetry measurement was carried out to study the oxidation reduction reactions of non-aqueous lead ions at various molar concentrations which is from 0.01M to 0.09M. Elecrochemical studies were carried out with Ag/AgCl as a reference electrode , Pt as working electrode while platinum mesh as counter electrode.Lead oxide appears to be poisonous yellow or reddish yellow solid. Structural characterization of films was analyze with X- ray diffraction (XRD) and optical band gap was determined by UV-Vis Spectroscopy.

https://www.materialsciencejournal.org/vol15no2/spray-pyrolysis-technique-for-the-deposition-of-lead-oxide-pbo-thin-films-its-electrochemical-behaviour-and-structural-and-optical-properties/ Oxidation Pb(NO3)2 Tafel UV UV-Vis Voltammetry XRD.