The present describes and structural features of some chelates polymers of Azelody bis-p-toyl carbamide (AZBPU) with first transition series metal ions viz Mn(II), Co (II), Ni(II) and Zn(II). The resultig chelate polymers have been characterized on the basis of elemental analysis, electronics spectral and magnetic suscetibility studies. The nature of bonding has been discussed on the basis of IR spectral data. To ascertain there thermal stability a detailed thermal studies was carried out by Freeman-Carol and Sharm-Went worth method.