In the present paper, we describe the synthesis and characterization of metal complexes of Hg (II) and Ag (I) using Schiff base ligand salicyldehydefurosemide. Furosemide (FSD) is a diuretic drug and it is used to increase the rate of urination through kidneys. Analytical data and stoichiometry suggest ligand metal ratio as 2:1 for Hg complex and 1 : 1 for Ag complex. The structure assigned to the complexes, synthesized via Schiff base formation is supported by infra-red spectral studies.