A compound CuNiTiO4 is prepared by solid diffusion method in the laboratory using standard chemical crystallographic of CuNiTiO₄. The magnetic susceptibility of compound is measured by Gauy’s method. The molar susceptibility is obtained with curie molar constant with respect to temperature. The Magnetic properties are studied under which the variation of Magnetic susceptibility with respect to temperature. The compound is found to be paramagnetic at room temperature. The paramagnetic behaviour is studied by plotting 1/Κ_m, vs temperature.