Three different procedures are reported for the synthesis of silica nanosphere. In all the method either agglomeration time, addition of hetero atom or use of surfactants plays a vital role. In absence of it give a full fledged crystal. This method is applicable to, irrespect of template, aluminium and silica source. The particles are in nanosphere with size in range from 100 to 500 nm. It is a convenient procedure than the conventional non-aqueous media synthesis.