eng Oriental Scientific Publishing Company Material Science Research India 0973-3469 2012-12-08 9 2 191 195 1101 article Preparation and Characterization of the Schiff Base Ligand (E)- N-(3-nitrobenzylidene) isonicotinohydrazide and its Silver (I) Complex [Ag(NNBIH)2]+ Shahriar Ghammamy 1 Sajjad Sedaghat 1 Department of Chemistry, Faculty of Science, Islamic Azad University, Malard Branch, Malard, Iran

We describe the synthesis and characterization of a new silver (I) complex of the Schiff base ligand (E) - N-(3-nitrobenzylidene) is onicotinohydrazide that abbreviated as NNBIH was synthesized and characterized. Ag (I) Metal complex of this Schiff base ligand prepared by reaction of nitrate salt of Ag (I) with NNBIH. Characterization of the ligand was made by microanalyses, FT-IR, UV–Visible spectroscopy and its complex was made by microanalyses, FT-IR and UV–Visible spectroscopy. TG- DTA and other analytical methods have been applied to the investigation of the thermal behavior and Structure of the compound [Ag(NNBIH)2]+. Thermal decomposition of these compounds is multistage processes.

 https://www.materialsciencejournal.org/vol9no2/preparation-and-characterization-of-the-schiff-base-ligand-e-n-3-nitrobenzylidene-isonicotinohydrazide-and-its-silver-i-complex-agnnbih2/ (E)-N-(3-nitrobenzylidene) isonicotinohydrazide Ag(I) complex Synthesis Thermal analysis