X-Ray Powder Diffraction and Thermal Studies on Copper (Ii) and Nickel (II) Complexes Using Schiff Base Derived from 2-Phenyl-3-{[(1E)-1-(2-Oxo-2H-Benzo[F]Chromen-3-Yl) Ethylidene] Amino}Quinazolin-4(3H)-One

Abstract
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Introduction
Materials and Methods
Results
Discussion
Conclusion
Acknowledgement
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Conflict of Interest
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References

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X-Ray Powder Diffraction and Thermal Studies on Copper (Ii) and Nickel (II) Complexes Using Schiff Base Derived from 2-Phenyl-3-{[(1E)-1-(2-Oxo-2H-Benzo[F]Chromen-3-Yl) Ethylidene] Amino}Quinazolin-4(3H)-One

Volume 5, Number 1

Tukaram Reddy¹, P. Chandrakant Reddy², M. Mallikarjun¹ and K. Siddappa¹*

¹Department of Chemistry Gulbarga University Gulbarga 585 106 (India)

²Department of Chemistry C.B.Degree College, Bhalki, Bidar (India)

DOI : http://dx.doi.org/10.13005/msri/050125

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ABSTRACT:

The Cu (II), Ni (II) complexes of Schiff bases derived from 2-Phenyl-3-{[(1E)-1-(3-oxo-3H-benzo[h]chromen-3-yl)ethylidene]amino}quinazolin-4(3H)-one have been synthesized and characterized by analytical data. The complexes are monomeric, possess in 1:2 (metal: ligand) stoichiometry and are non-electrolytic in nature. The Cu (II) complexes have been characterized by thermal analysis and X-ray diffractometry. The ligand and its Ni(II) complex have been characterized by powder X-ray diffraction. The thermal analysis of Ni (II) complex has also been carried out.

KEYWORDS:

Cu (II); Ni (II) complexes; Schiff base; X-ray powder diffraction

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